syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

Base Information

Chemical Name:syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten
CAS No.:82265-64-3
Molecular Formula:C₂₃H₁₉O₉PW
Molecular Weight:654.222
Hs Code.:

Synonyms:syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

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Chemical Property of syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

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Technology Process of syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

There total 1 articles about syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 74363-95-4
(3,4-dimethyl-1-phenylphosphole)pentacarbonyltungsten

: 762-42-5
dimethyl acetylenedicarboxylate

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

Guidance literature:: In toluene; W complex and org. compd. heated at 90°C for 24 h in toluene under Ar; evapn., chromy. (SiO2, toluene) under Ar; elem. anal.;

Reference yield: 95.0%

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 88081-26-9,88000-31-1
(9-phenyl-9-phosphabicyclo[6.1.0]nonane)pentacarbonyltungsten

Guidance literature:: copper(l) chloride; In toluene; The soln. of reagents in toluene was heated at 55°C for 3 h (Ar atm.);; evapd., chromd. on silica column with hexane under Ar atm.; the mixt. of isomers was obtained;;
DOI:10.1021/om00081a021

Reference yield: 92.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 88000-32-2,88080-15-3
(1,2-diphenylphosphirane)pentacarbonyltungsten

Guidance literature:: copper(l) chloride; In toluene; The soln. of reagents in toluene was heated at 55°C for 3 h (Ar atm.);; evapd., chromd. on silica column with hexane under Ar atm.; the mixt. of isomers was obtained;;
DOI:10.1021/om00081a021