trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride

Base Information

Chemical Name:trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride
CAS No.:1450842-81-5
Molecular Formula:C₆₆H₉₅F₃O₉
Molecular Weight:1089.47
Hs Code.:

Synonyms:trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride

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Chemical Property of trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride

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Technology Process of trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride

There total 2 articles about trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 110934-58-2
3,4,5-tris(4-dodecyloxybenzyloxy)benzoic acid

: 407-25-0
trifluoroacetic anhydride

: 1450842-81-5
trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride

Guidance literature:: In chloroform; at 20 ℃; for 0.25h;
DOI:10.1016/j.polymer.2013.07.027

Reference yield:

: 118468-31-8
methyl 3,4,5-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzoate

: 1450842-81-5
trifluoroacetic 3,4,5-tris[4-(n-dodecan-1-yloxy)benzyloxy]benzoic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; water / tetrahydrofuran; ethanol / 0.5 h / Reflux

2: chloroform / 0.25 h / 20 °C

With water; potassium hydroxide; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/j.polymer.2013.07.027