methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate

Base Information

Chemical Name:methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate
CAS No.:194608-84-9
Molecular Formula:C₂₄H₂₉ClO₅S
Molecular Weight:465.01
Hs Code.:

Synonyms:methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate

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Chemical Property of methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate

Chemical Property:

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Technology Process of methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate

There total 8 articles about methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-bromo-3-(2-hydroxy-3-propyl-4-propionyl)-phenoxy)propane

: 91361-78-3
3-chloro-4-dimethylcarbamoylthio-phenylacetic acid methyl ester

: 194608-84-9
methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate

Guidance literature:: With sodium methylate; In methanol; dichloromethane;

Reference yield:

: 5792-36-9
2',4'-dihydroxypropiophenone

: 194608-84-9
methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: Cs₂CO₃ / dimethylformamide / 20 °C

2: 1,2-dichloro-benzene / Heating

3: 100 percent / H₂ / 5 percent Pd/C / various solvent(s) / 760 Torr

4: Cs₂CO₃ / dimethylformamide

With hydrogen; caesium carbonate; palladium on activated charcoal; In N,N-dimethyl-formamide; 1,2-dichloro-benzene; 2: Claisen rearrangement;
DOI:10.1016/S0960-894X(03)00115-X

Reference yield:

: 74815-88-6
2,4-dihydroxy-3-allylpropiophenone

: 194608-84-9
methyl 3-chloro-4-(3-(2-propyl-3-hydroxy-4-propionylphenoxy)propylthio)phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 5 percent Pd/C / various solvent(s) / 760 Torr

2: Cs₂CO₃ / dimethylformamide

With hydrogen; caesium carbonate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(03)00115-X