2,4-dichloro-4'-hydroxydiphenylmethane

Base Information

• Chemical Name: 2,4-dichloro-4'-hydroxydiphenylmethane
• CAS No.: 57836-47-2
• Molecular Formula: C₁₃H₁₀Cl₂O
• Molecular Weight: 253.128

Synonyms:2,4-dichloro-4'-hydroxydiphenylmethane

Chemical Property of 2,4-dichloro-4'-hydroxydiphenylmethane

Chemical Property:

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Technology Process of 2,4-dichloro-4'-hydroxydiphenylmethane

There total 1 articles about 2,4-dichloro-4'-hydroxydiphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-Dichlorobenzyl chloride (94-99-5) + phenol (108-95-2,27073-41-2) → 2,4-dichloro-2'-hydroxydiphenylmethane + 2,4-dichloro-4'-hydroxydiphenylmethane (57836-47-2)

Guidance literature:

Envirocat EPZ₁₀; for 0.583333h; Heating;

DOI:10.1007/s007060070069

Reference yield:

ethyl (S)-α-(4-methyl-phenylsulphonyloxy)-propionate (33798-77-5) + 2,4-dichloro-4'-hydroxydiphenylmethane (57836-47-2) → D-(+)-2-[4-(2,4-dichlorobenzyl)-phenoxy]-propionic acid ethyl ester (57836-50-7)

Guidance literature:

With potassium carbonate; In acetonitrile;

Reference yield:

2-aminopyridine (504-29-0) + 6-chloromethyl-3,4-dimethyl-2-pyrone (15085-89-9) + 2,4-dichloro-4'-hydroxydiphenylmethane (57836-47-2) → 6-[4-(2,4-dichlorobenzyl)phenoxymethyl]-1-hydroxy-3,4-dimethyl-2-pyridone

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In N-methyl-acetamide; dichloromethane; water;

upstream raw materials:

2,4-Dichlorobenzyl chloride

phenol

Downstream raw materials:

4-[4-(2,4-Dichloro-benzyl)-phenoxy]-butyric acid ethyl ester

α-[4-(2,4-dichlorobenzyl)-phenoxy]-propionic acid methyl ester

2-[4-(2,4-Dichloro-benzyl)-phenoxy]-butyric acid ethyl ester

2-[4-(2,4-Dichloro-benzyl)-phenoxy]-propionitrile

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