3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon

Base Information

Chemical Name:3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon
CAS No.:98909-45-6
Molecular Formula:C₁₇H₂₂O₃
Molecular Weight:274.36
Hs Code.:

Synonyms:3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon

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Chemical Property of 3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon

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Technology Process of 3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon

There total 1 articles about 3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 98909-40-1
3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-1-phenyl-1-propanon

: 98909-45-6
3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon

Guidance literature:: With potassium hydroxide; tetra-(n-butyl)ammonium iodide; dicyclohexyl-carbodiimide; copper(l) chloride; Yield given. Multistep reaction; 1.) THF, H₂O, r.t., 2.) THF, 20 h, reflux;

Reference yield: 74.0%

: 98-01-1
furfural

: 98909-45-6
3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon

: 98909-51-4
3-Benzoyl-4-(2-ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-1-(2-furyl)-1-butanon

Guidance literature:: With triethylamine; HEMET(+) Br(-); In ethanol; at 80 ℃; for 16h;

Reference yield:

: 98909-45-6
3-(2-Ethyl-4,5-dimethyl-1,3-dioxolan-2-yl)-2-methylen-1-phenyl-1-propanon

: 98909-70-7
3-Benzoyl-1-(2-furyl)-1,5-heptandion

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / Et₃N / HEMET(+) Br(-) / ethanol / 16 h / 80 °C

2: 91 percent / CH₃COOH / 5 h / 70 °C

With acetic acid; triethylamine; HEMET(+) Br(-); In ethanol;