benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

• Chemical Name: benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside
• CAS No.: 863914-96-9
• Molecular Formula: C₁₁₈H₁₀₆O₃₀
• Molecular Weight: 2004.12

Synonyms:benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property of benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property:

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Technology Process of benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 2 articles about benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

benzyl 2-O-[(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside (863914-95-8) + 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate → benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside (863914-96-9)

Guidance literature:

benzyl 2-O-[(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside; 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate; In 1,2-dichloro-ethane; at 0 ℃; for 0.666667h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 0 ℃;

With triethylamine; In 1,2-dichloro-ethane; at 0 ℃;

Reference yield: 94.0%

benzyl 2-O-[(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside (863914-95-8) + 3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranoside trichloroacetimidate (431981-80-5) → benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside (863914-96-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 0 ℃; for 0.166667h;

DOI:10.1016/j.bmc.2007.10.044

Reference yield: 64.0%

benzyl 2-O-[(3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside (863914-96-9) → benzyl 2-O-[(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside (863914-97-0)

Guidance literature:

With methanol; palladium dichloride; In 1,2-dichloro-ethane; at 70 ℃; for 0.666667h;

DOI:10.1016/j.bmc.2007.10.044

upstream raw materials:

benzyl 2-O-[(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside

3-O-allyl-2,4,6-tri-O-benzoyl-α-D-mannopyranoside trichloroacetimidate

Downstream raw materials:

benzyl 2-O-[(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-D-mannopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-α-Dmannopyranosyl)]-3,4,6-tri-O-benzyl-α-D-mannopyranoside

benzyl (3-O-allyl-α-D-mannopyranosyl)-(1->3)-(α-D-mannopyranosyl)-(1->3)-(α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranoside)

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