N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

Base Information

Chemical Name:N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine
CAS No.:102226-97-1
Molecular Formula:C₂₄H₃₃N₃O₃
Molecular Weight:411.544
Hs Code.:

Synonyms:N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

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Chemical Property of N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

Chemical Property:

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Technology Process of N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

There total 5 articles about N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4742-01-2
N-(3-aminopropyl)aniline

: 85175-65-1
7,8-dimethoxy-3-(3-chloropropyl)-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

: 102226-97-1
N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

Guidance literature:: triethylamine;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 102226-97-1
N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / dichloromethane

2: triethylamine / dichloromethane

3: hydrogenchloride; acetic acid

4: potassium tert-butylate / dimethyl sulfoxide; acetone

5: palladium/charcoal; water; acetic acid

6: triethylamine

With thionyl chloride; potassium tert-butylate; triethylamine; triethylamine; In hydrogenchloride; palladium/charcoal; dichloromethane; water; acetic acid; dimethyl sulfoxide; acetone;

Reference yield:

: 73954-34-4
N-(2,2-dimethoxy-ethyl)-3,4-dimethoxyphenylacetamide

: 102226-97-1
N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; acetic acid

2: potassium tert-butylate / dimethyl sulfoxide; acetone

3: palladium/charcoal; water; acetic acid

4: triethylamine

With potassium tert-butylate; triethylamine; In hydrogenchloride; palladium/charcoal; water; acetic acid; dimethyl sulfoxide; acetone;