Technology Process of N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine
There total 7 articles about N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride; paraformaldehyde;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: thionyl chloride / dichloromethane
2: triethylamine / dichloromethane
3: hydrogenchloride; acetic acid
4: potassium tert-butylate / dimethyl sulfoxide; acetone
5: palladium/charcoal; water; acetic acid
6: triethylamine
7: sodium cyanoborohydride; paraformaldehyde
With
thionyl chloride; potassium tert-butylate; sodium cyanoborohydride; triethylamine; paraformaldehyde;
triethylamine;
In
hydrogenchloride; palladium/charcoal; dichloromethane; water; acetic acid; dimethyl sulfoxide; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate / dimethyl sulfoxide; acetone
2: palladium/charcoal; water; acetic acid
3: triethylamine
4: sodium cyanoborohydride; paraformaldehyde
With
potassium tert-butylate; sodium cyanoborohydride; paraformaldehyde;
triethylamine;
In
palladium/charcoal; water; acetic acid; dimethyl sulfoxide; acetone;