N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine

Base Information

Chemical Name:N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine
CAS No.:102226-96-0
Molecular Formula:C₂₅H₃₅N₃O₃
Molecular Weight:425.571
Hs Code.:

Synonyms:N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine

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Chemical Property of N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine

Chemical Property:

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Technology Process of N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine

There total 7 articles about N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102226-97-1
N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-3-(phenylamino)-propylamine

: 102226-96-0
N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine

Guidance literature:: With sodium cyanoborohydride; paraformaldehyde;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 102226-96-0
N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / dichloromethane

2: triethylamine / dichloromethane

3: hydrogenchloride; acetic acid

4: potassium tert-butylate / dimethyl sulfoxide; acetone

5: palladium/charcoal; water; acetic acid

6: triethylamine

7: sodium cyanoborohydride; paraformaldehyde

With thionyl chloride; potassium tert-butylate; sodium cyanoborohydride; triethylamine; paraformaldehyde; triethylamine; In hydrogenchloride; palladium/charcoal; dichloromethane; water; acetic acid; dimethyl sulfoxide; acetone;

Reference yield:

: 73942-87-7
7,8-Dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one

: 102226-96-0
N-[3-(7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-N-(3-phenylaminopropyl)-methylamine

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tert-butylate / dimethyl sulfoxide; acetone

2: palladium/charcoal; water; acetic acid

3: triethylamine

4: sodium cyanoborohydride; paraformaldehyde

With potassium tert-butylate; sodium cyanoborohydride; paraformaldehyde; triethylamine; In palladium/charcoal; water; acetic acid; dimethyl sulfoxide; acetone;