Technology Process of 1,3-Dipropyl-8-phenylxanthine
There total 11 articles about 1,3-Dipropyl-8-phenylxanthine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine;
In
1,2-dimethoxyethane;
at 50 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: glacial acetic acid / ethanol / Ambient temperature
2: 90 percent / iodine / 1,2-dimethoxy-ethane / 4 h / 50 °C
With
iodine; acetic acid;
In
1,2-dimethoxyethane; ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NaNO2, AcOH / H2O / 90 °C
2: H2 / 5percent Pd/C / ethanol / 24 h / 3102.9 Torr
3: AcOH / ethanol / Heating
4: diethyl azodicarboxylate / 1,2-dimethoxy-ethane / 0.5 h / Heating
With
hydrogen; acetic acid; sodium nitrite; diethylazodicarboxylate;
palladium on activated charcoal;
In
1,2-dimethoxyethane; ethanol; water;
DOI:10.1021/jm00108a029
