alcohol

Base Information

Chemical Name:alcohol
CAS No.:442663-47-0
Molecular Formula:C₄₅H₅₄IN₃O₁₂
Molecular Weight:955.841
Hs Code.:

Synonyms:alcohol

Suppliers and Price of alcohol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 11 raw suppliers

Chemical Property of alcohol

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of alcohol

There total 27 articles about alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 442663-29-8
(2-(3-benzyloxy-2-iodo-4-methoxy-5-methyl-phenyl)-1-{[2-(tert-butyl-diphenyl-silanyloxy)-1-(6-methoxymethoxy-7-methyl-benzo[1,3]dioxol-4-yl)-ethyl]-[1-(4-methoxy-phenylcarbamoyl)-ethyl]-carbamoyl}-ethyl)-carbamic acid tert-butyl ester

: 442663-47-0
alcohol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/ja026216d

Reference yield:

: 533-31-3
Sesamol

: 442663-47-0
alcohol

Guidance literature:: Multi-step reaction with 11 steps

1.1: NaH / tetrahydrofuran; dimethylformamide; various solvent(s) / 0 - 20 °C

1.2: 97 percent / tetrahydrofuran; dimethylformamide; various solvent(s) / 0 - 20 °C

2.1: n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

2.2: 92 percent / aq. H₂O₂; trimethylboronate; AcOH / tetrahydrofuran; hexane / 4.5 h / 20 °C

3.1: 89 percent / TFA / CH₂Cl₂ / 2.17 h / -10 °C

4.1: 90 percent / pyridine / CH₂Cl₂ / 0.08 h / 0 °C

5.1: 85 percent / NaBH₄ / methanol / 0.5 h / 0 °C

6.1: 91 percent / imidazole / dimethylformamide / 20 °C

7.1: 97 percent / PdCl₂(dppf) / tetrahydrofuran / 4.5 h / Heating

8.1: Pb(OAc)4 / acetonitrile / 0 °C

9.1: 436 mg / NH₂OH*HCl; NaOAc / ethanol / 1.5 h / 20 °C

10.1: 90 percent / methanol / 1 h / Heating

11.1: 89 percent / TBAF / tetrahydrofuran / 0.5 h / 20 °C

With pyridine; 1H-imidazole; lead(IV) acetate; sodium tetrahydroborate; n-butyllithium; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium acetate; sodium hydride; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 3.1: Mannich reaction / 10.1: Ugi reaction;
DOI:10.1021/ja026216d

Reference yield:

: 111726-43-3
3,4-(methylenedioxy)phenyl methoxymethyl ether

: 442663-47-0
alcohol

Guidance literature:: Multi-step reaction with 10 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

1.2: 92 percent / aq. H₂O₂; trimethylboronate; AcOH / tetrahydrofuran; hexane / 4.5 h / 20 °C

2.1: 89 percent / TFA / CH₂Cl₂ / 2.17 h / -10 °C

3.1: 90 percent / pyridine / CH₂Cl₂ / 0.08 h / 0 °C

4.1: 85 percent / NaBH₄ / methanol / 0.5 h / 0 °C

5.1: 91 percent / imidazole / dimethylformamide / 20 °C

6.1: 97 percent / PdCl₂(dppf) / tetrahydrofuran / 4.5 h / Heating

7.1: Pb(OAc)4 / acetonitrile / 0 °C

8.1: 436 mg / NH₂OH*HCl; NaOAc / ethanol / 1.5 h / 20 °C

9.1: 90 percent / methanol / 1 h / Heating

10.1: 89 percent / TBAF / tetrahydrofuran / 0.5 h / 20 °C

With pyridine; 1H-imidazole; lead(IV) acetate; sodium tetrahydroborate; n-butyllithium; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium acetate; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2.1: Mannich reaction / 9.1: Ugi reaction;
DOI:10.1021/ja026216d