4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate

Base Information

Chemical Name:4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate
CAS No.:1446029-50-0
Molecular Formula:C₃₁H₃₃BrO₅
Molecular Weight:565.504
Hs Code.:

Synonyms:4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate

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Technology Process of 4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate

There total 4 articles about 4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 20769-85-1
2-bromoisobutyric acid bromide

: 1446029-49-7
4-(4-(2-(4-(allyloxy)phenyl)5-hydroxypentan-2-yl)phenoxy)benzaldehyde

: 1446029-50-0
4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate

Guidance literature:: With triethylamine; at 0 - 20 ℃; for 14.5h;
DOI:10.1002/pola.26598

Reference yield:

: 93727-83-4
4,4'-(5-hydroxypentane-2,2-diyl)diphenol

: 1446029-50-0
4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 0.17 h / Reflux

1.2: 8.5 h / Reflux

2.1: potassium carbonate / 0.17 h / Reflux

2.2: 8.5 h / 100 °C

3.1: triethylamine / 14.5 h / 0 - 20 °C

With potassium carbonate; triethylamine; In acetone;
DOI:10.1002/pola.26598

Reference yield:

: 7297-85-0
4-hydroxy-γ-(4-hydroxyphenyl)-γ-methyl-benzenebutanoic acid methyl ester

: 1446029-50-0
4-(4-(allyloxy)phenyl)-4-(4-(4-formylphenoxy)phenyl)pentyl 2-bromo-2-methylpropanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / Reflux

2.1: potassium carbonate / acetone / 0.17 h / Reflux

2.2: 8.5 h / Reflux

3.1: potassium carbonate / 0.17 h / Reflux

3.2: 8.5 h / 100 °C

4.1: triethylamine / 14.5 h / 0 - 20 °C

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; acetone;
DOI:10.1002/pola.26598