bis(5-methyl-2-thienyl)iodonium hexafluorophosphate

Base Information

• Chemical Name: bis(5-methyl-2-thienyl)iodonium hexafluorophosphate
• CAS No.: 1190072-86-6
• Molecular Formula: C₁₀H₁₀IS₂*F₆P
• Molecular Weight: 466.19
• Mol file: 1190072-86-6.mol

Synonyms:bis(5-methyl-2-thienyl)iodonium hexafluorophosphate

Chemical Property of bis(5-methyl-2-thienyl)iodonium hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of bis(5-methyl-2-thienyl)iodonium hexafluorophosphate

There total 1 articles about bis(5-methyl-2-thienyl)iodonium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(5-methyl-2-thienyl)iodonium trifluoroacetate (1190072-80-0) → 2-iodo-5-methylthiophene (16494-36-3) + 5-methyl-3H-thiophen-2-one (930-64-3) + bis(5-methyl-2-thienyl)iodonium hexafluorophosphate (1190072-86-6)

Guidance literature:

With ammonium hexafluorophosphate; water;

DOI:10.1016/j.jfluchem.2009.02.001

Reference yield: 95.0%

bis(5-methyl-2-thienyl)iodonium hexafluorophosphate (1190072-86-6) + 2,7-diazadibenzophosphole oxide (1333225-60-7) → N,N'-bis(5-methyl-2-thienyl)-2,7-diazadibenzophosphole oxide di(hexafluorophosphate)

Guidance literature:

With copper(II) acetate monohydrate; In N,N-dimethyl-formamide; at 40 ℃; for 36h; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.5b06413

upstream raw materials:

bis(5-methyl-2-thienyl)iodonium trifluoroacetate

Refernces