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Technology Process of [Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6)

[Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6)

Base Information
  • Chemical Name:[Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6)
  • CAS No.:260781-73-5
  • Molecular Formula:C31H24F4NPRh*F6P
  • Molecular Weight:765.375
  • Hs Code.:
[Rh(tetrafluorobenzobarrelene)(P(CH<sub>2</sub>CH<sub>2</sub>Py)Ph<sub>2</sub>)](PF<sub>6</sub>)

Synonyms:[Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6)

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Chemical Property of [Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6)
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Technology Process of [Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6)

There total 1 articles about [Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

ammonium hexafluorophosphate

ammonium hexafluorophosphate

[Rh2(μ-Cl)2(tetrafluorobenzobarrelene)2]

[Rh2(μ-Cl)2(tetrafluorobenzobarrelene)2]

2-(2-(diphenylphosphino)ethyl)pyridine
10150-27-3

2-(2-(diphenylphosphino)ethyl)pyridine

[Rh(tetrafluorobenzobarrelene)(P(CH<sub>2</sub>CH<sub>2</sub>Py)Ph<sub>2</sub>)](PF<sub>6</sub>)
260781-73-5

[Rh(tetrafluorobenzobarrelene)(P(CH2CH2Py)Ph2)](PF6)

Guidance literature:
With AgNO3; In ethanol; acetone; byproducts: AgCl; under N2 atm. to stirred suspn. of Rh-complex in acetone were added ligand and AgNO3 and stirred for 24 h, AgCl was filtered off, acetone was evapd., ethanol was aded, NH4PF6 in ethanol was added; filtration, washed with CHCl3 and vac.-dried; elem. anal.;
DOI:10.1021/ic990634a
upstream raw materials:

2-(2-(diphenylphosphino)ethyl)pyridine

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