tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

Base Information

Chemical Name:tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane
CAS No.:460323-55-1
Molecular Formula:C₂₂H₃₆OSi
Molecular Weight:344.613
Hs Code.:

<i>tert</i>-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

Synonyms:tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

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Chemical Property of tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

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Technology Process of tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

There total 9 articles about tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 147821-59-8
(S)-4-(3,7-dimethylocta-1,6-dien-3-yl)phenol

: 460323-55-1
tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4039(02)00857-2

Reference yield:

: 143590-14-1
(R)-2-(4-methoxyphenyl)propan-1-ol

: 460323-55-1
tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

Guidance literature:: Multi-step reaction with 8 steps

1.1: 93 percent / pyridine / CH₂Cl₂ / 20 °C

2.1: 89 percent / dimethylsulfoxide / 80 °C

3.1: DIBAL / toluene / 20 °C

4.1: BuLi / tetrahydrofuran / 20 °C

5.1: KOH / H₂O; methanol / 20 °C

6.1: DPPA; Et₃N / toluene / 20 °C

6.2: HCl / H₂O

7.1: 95 percent / 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 0 °C

With pyridine; potassium hydroxide; n-butyllithium; 2,6-di-tert-butyl-4-methylpyridine; diphenyl-phosphinic acid; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; 4.1: Wordsworth-Emmons reaction / 6.1: Curtius rearrangement;
DOI:10.1016/S0040-4039(02)00857-2

Reference yield:

: 460323-57-3
Acetic acid (R)-2-(4-methoxy-phenyl)-propyl ester

: 460323-55-1
tert-butyl-[4-(1,5-dimethyl-1-vinyl-hex-4-enyl)-phenoxy]-dimethyl-silane

Guidance literature:: Multi-step reaction with 9 steps

1.1: 97 percent / KOH / methanol; H₂O / 20 °C

2.1: 93 percent / pyridine / CH₂Cl₂ / 20 °C

3.1: 89 percent / dimethylsulfoxide / 80 °C

4.1: DIBAL / toluene / 20 °C

5.1: BuLi / tetrahydrofuran / 20 °C

6.1: KOH / H₂O; methanol / 20 °C

7.1: DPPA; Et₃N / toluene / 20 °C

7.2: HCl / H₂O

8.1: 95 percent / 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 0 °C

With pyridine; potassium hydroxide; n-butyllithium; 2,6-di-tert-butyl-4-methylpyridine; diphenyl-phosphinic acid; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; 5.1: Wordsworth-Emmons reaction / 7.1: Curtius rearrangement;
DOI:10.1016/S0040-4039(02)00857-2