tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

Base Information

Chemical Name:tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate
CAS No.:152898-89-0
Molecular Formula:C₁₆H₂₉NO₄
Molecular Weight:299.411
Hs Code.:

Synonyms:tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

Suppliers and Price of tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

There total 6 articles about tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 52719-94-5
(1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl carbamate

: 152898-89-0
tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1021/jo070614n

Reference yield:

: 152899-01-9
C₂₄H₃₇NO₅

: 152898-89-0
tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; for 1h; Yield given;
DOI:10.1021/jo00077a068

Reference yield:

: 2216-51-5
(-)-menthol

: 152898-89-0
tert-butyl (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl imidodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / CCl₄ / 6 h / 55 - 60 °C

2: 100 percent / aq. NH₃ / tetrahydrofuran; H₂O / 20 °C

3: 40 percent / NaH / tetrahydrofuran / 0.25 h / 0 °C

With pyridine; ammonium hydroxide; sodium hydride; In tetrahydrofuran; tetrachloromethane; water;
DOI:10.1021/jo070614n