(E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester

Base Information

Chemical Name:(E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester
CAS No.:1437306-80-3
Molecular Formula:C₂₀H₂₉N₃O₇
Molecular Weight:423.466
Hs Code.:

Synonyms:(E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester

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Chemical Property of (E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester

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Technology Process of (E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester

There total 1 articles about (E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1135-24-6,537-98-4
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 1437306-80-3
(E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 0 - 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 80 °C

With thionyl chloride; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/bc400074w

Reference yield: 47.0%

: 1437306-80-3
(E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester

: 1271743-28-2
(E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 5h;
DOI:10.1021/bc400074w

Reference yield:

: 1437306-80-3
(E)-3-(4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-methoxyphenyl)acrylic acid ethyl ester

: 1437306-74-5
C₃₃H₄₆N₄O₁₂

Guidance literature:: Multi-step reaction with 6 steps

1: lithium hydroxide / tetrahydrofuran; methanol; water / 5 h / 20 °C

2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; TBTU / N,N-dimethyl-formamide; water / 23.5 h / 20 °C

3: dichloromethane / 0 - 20 °C

4: triethylamine / dichloromethane / 0 - 20 °C

5: triphenylphosphine; water / tetrahydrofuran / 48 h / 20 °C

6: potassium hydroxide; hydroxylamine hydrochloride / methanol / 24 h / 20 °C / Inert atmosphere

With TBTU; hydroxylamine hydrochloride; water; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 5: |Staudinger Azide Reduction;
DOI:10.1021/bc400074w