5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde

Base Information

Chemical Name:5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde
CAS No.:1142946-85-7
Molecular Formula:C₁₉H₁₄ClN₃O₃S₂
Molecular Weight:431.923
Hs Code.:

Synonyms:5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde

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Chemical Property of 5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde

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Technology Process of 5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde

There total 1 articles about 5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 934524-10-4
2,4-dichloro-7-p-methylbenzenesulfonyl-7H-pyrrole[2,3-d]pyrimidin-4-amine

: 3-methyl-5- (4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophene-2-carbaldehyde

: 1142946-85-7
5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde

Guidance literature:: With potassium carbonate; dichloro[1,1'-bis(di-t-butylphosphino)ferrocene]palladium(II); In N,N-dimethyl-formamide; at 110 ℃; for 1.58333h; Microwave irradiation;

Reference yield: 64.0%

: 1142946-85-7
5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde

: 123207-48-7
3-[(4-morpholinyl)methyl]aniline

: 1142948-04-6
C₃₀H₂₉N₅O₄S₂

Guidance literature:: With tri-tert-butyl phosphine; triethylamine; palladium diacetate; In N,N-dimethyl-formamide; toluene; at 160 ℃; for 0.75h; Microwave irradiation;

Reference yield: 64.0%

: 16153-81-4
4-(4-Methyl-piperazino)-anilin

: 1142946-85-7
5-{2-chloro-7-[(4-methylphenyl)sulfonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-yl}-3-methylthiophene-2-carbaldehyde

: 1142948-02-4
C₃₀H₃₀N₆O₃S₂

Guidance literature:: With tri-tert-butyl phosphine; triethylamine; palladium diacetate; In N,N-dimethyl-formamide; toluene; at 160 ℃; for 0.416667 - 0.75h; Product distribution / selectivity; Microwave irradiation;