1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline

Base Information

Chemical Name:1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline
CAS No.:1325720-01-1
Molecular Formula:C₂₄H₂₇ClN₄
Molecular Weight:406.958
Hs Code.:

Synonyms:1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline

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Chemical Property of 1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline

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Technology Process of 1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline

There total 5 articles about 1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₅ClN₄

: 1325720-01-1
1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline

Guidance literature:: With sodium cyanoborohydride; In methanol; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2011.08.027

Reference yield:

: 1339940-11-2
9-(3-chlorobenzyl)-β-carboline-1-carboxaldehyde

: 1325720-01-1
1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; dichloromethane / 20 °C

2: sodium cyanoborohydride / methanol / 24 h / 0 - 20 °C

With sodium cyanoborohydride; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.08.027

Reference yield:

: 1339940-08-7
9-(3-chlorobenzyl)-1-methyl-β-carboline

: 1325720-01-1
1-[N-(3-dimethylamino-propyl)-aminomethyl]-9-(3-chlorobenzyl)-β-carboline

Guidance literature:: Multi-step reaction with 3 steps

1: selenium(IV) oxide / 1,4-dioxane / 2 h / Reflux

2: methanol; dichloromethane / 20 °C

3: sodium cyanoborohydride / methanol / 24 h / 0 - 20 °C

With selenium(IV) oxide; sodium cyanoborohydride; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.08.027