N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Base Information

Chemical Name:N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide
CAS No.:1567401-79-9
Molecular Formula:C₂₉H₂₆IN₃O₂
Molecular Weight:575.449
Hs Code.:

Synonyms:N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

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Chemical Property of N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

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Technology Process of N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

There total 4 articles about N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1567401-76-6
C₂₉H₂₇I₂N₃O₂

: 1567401-79-9
N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Guidance literature:: With copper(l) iodide; potassium carbonate; L-proline; In dimethyl sulfoxide; at 80 ℃; for 0.666667h; Microwave irradiation; Inert atmosphere; Sealed tube;
DOI:10.1021/co4001309

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 1567401-79-9
N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 72 h / 20 °C

2: copper(l) iodide; L-proline; potassium carbonate / dimethyl sulfoxide / 0.67 h / 80 °C / Microwave irradiation; Inert atmosphere; Sealed tube

With copper(l) iodide; potassium carbonate; L-proline; In methanol; dimethyl sulfoxide; 1: |Ugi Condensation;
DOI:10.1021/co4001309

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 1567401-79-9
N-cyclohexyl-6-(2-iodophenyl)-5-oxo-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 72 h / 20 °C

2: copper(l) iodide; L-proline; potassium carbonate / dimethyl sulfoxide / 0.67 h / 80 °C / Microwave irradiation; Inert atmosphere; Sealed tube

With copper(l) iodide; potassium carbonate; L-proline; In methanol; dimethyl sulfoxide; 1: |Ugi Condensation;
DOI:10.1021/co4001309