5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one

Base Information

• Chemical Name: 5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one
• CAS No.: 92439-94-6
• Molecular Formula: C₁₄H₁₇N₃O
• Molecular Weight: 243.308

Synonyms:5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one

Chemical Property of 5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one

Chemical Property:

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Technology Process of 5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one

There total 1 articles about 5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H14O3NC6H5 (41276-30-6) → 5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one (92439-94-6)

Guidance literature:

Multi-step reaction with 2 steps

1: xylene / 8 h / Heating / reflux

2: hydrogen; acetic acid / palladium over charcoal / ethanol / 45 h / 2585.81 Torr

With hydrogen; acetic acid; palladium over charcoal; In ethanol; xylene;

Reference yield:

4-ethoxycyclohexan-1-one (23510-92-1) + 1,3-dihydro-5,6-dimethyl-1-(4-piperidinyl)-2H-benzimidazol-2-one (80119-44-4) + 5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one (92439-94-6) → cis-1-{1-[4-(ethyloxy)cyclohexyl]-4-piperidinyl}-5,6-dimethyl-1,3-dihydro-2H-benzimidazol-2-one + trans-1-{1-[4-(ethyloxy)cyclohexyl]-4-piperidinyl}-5,6-dimethyl-1,3-dihydro-2H-benzimidazol-2-one

Guidance literature:

4-ethoxycyclohexan-1-one; 1,3-dihydro-5,6-dimethyl-1-(4-piperidinyl)-2H-benzimidazol-2-one; 5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one; With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 114h;

With hydrogen; acetic acid; palladium 10% on activated carbon; In ethanol; for 20h; under 2585.81 Torr;

With sodium carbonate; In water;

Reference yield:

5,6-dimethyl-1-(1,2,3,6-tetrahydro-4-pyridinyl)-1,3-dihydro-2H-benzimidazol-2-one (92439-94-6) → cis-1-{1-[4-(ethyloxy)cyclohexyl]-4-piperidinyl}-5,6-dimethyl-1,3-dihydro-2H-benzimidazol-2-one

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogen; acetic acid / palladium over charcoal / ethanol / 2585.81 Torr

2.1: sodium tris(acetoxy)borohydride / dichloromethane / 114 h / 20 °C

2.2: 20 h / 2585.81 Torr

With hydrogen; sodium tris(acetoxy)borohydride; acetic acid; palladium over charcoal; In ethanol; dichloromethane;

upstream raw materials:

C₉H₁₄O₃NC₆H₅

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