potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

Base Information

Chemical Name:potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate
CAS No.:1397275-22-7
Molecular Formula:C₁₄H₂₀BF₃NO₃*K
Molecular Weight:357.222
Hs Code.:

Synonyms:potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

Suppliers and Price of potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

There total 4 articles about potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1396515-28-8
tert-butyl 2-methoxybenzyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

: 1397275-22-7
potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

Guidance literature:: With potassium hydrogen difluoride; In water; acetone; at 0 - 20 ℃; for 0.5h;
DOI:10.1021/ol301955s

Reference yield:

: 6850-57-3
2-methoxybenzylamine

: 1397275-22-7
potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 - 20 °C

2.2: 20 °C

3.1: potassium hydrogen difluoride / acetone; water / 0.5 h / 0 - 20 °C

With n-butyllithium; potassium hydrogen difluoride; In tetrahydrofuran; hexane; water; acetone;
DOI:10.1021/ol301955s

Reference yield:

: 153903-20-9
t-Butyl N-(2-methoxybenzyl)carbamate

: 1397275-22-7
potassium tert-butyl 2-methoxybenzyl{(trifluoroborato)methyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 - 20 °C

1.2: 20 °C

2.1: potassium hydrogen difluoride / acetone; water / 0.5 h / 0 - 20 °C

With n-butyllithium; potassium hydrogen difluoride; In tetrahydrofuran; hexane; water; acetone;
DOI:10.1021/ol301955s