6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin

Base Information

Chemical Name:6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin
CAS No.:1154758-60-7
Molecular Formula:C₅₀H₇₉N₇O₂₁
Molecular Weight:1114.21
Hs Code.:

Synonyms:6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin

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Chemical Property of 6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin

Chemical Property:

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Technology Process of 6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin

There total 13 articles about 6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1154758-59-4
6'-PNZ-2',3,3''-triBoc-sisomicin

: 52558-24-4
(s)-3-tert-butoxycarbonylamino-2-hydroxypropionic acid

: 1154758-60-7
6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin

Guidance literature:: (s)-3-tert-butoxycarbonylamino-2-hydroxypropionic acid; With N-hydroxy-5-norbomene-2,3-dicarboxylic acid imide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 2h;

6'-PNZ-2',3,3''-triBoc-sisomicin; In N,N-dimethyl-formamide;

Reference yield:

: C₁₇H₂₂N₂O₇

: 1154758-59-4
6'-PNZ-2',3,3''-triBoc-sisomicin

: 1154758-60-7
6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin

Guidance literature:: In N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1154758-60-7
6'-PNZ-2',3,3''-triBoc-1-(N-Boc-3-amino-2(S)-hydroxy-propionyl)-sisomicin

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine / tetrahydrofuran / 3 h

2: 2,2',2''-triaminotriethylamine / dichloromethane / 0.75 h

3: N,N-dimethyl-formamide

With 4-methyl-morpholine; 2,2',2''-triaminotriethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;