2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate

Base Information

Chemical Name:2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate
CAS No.:1327188-12-4
Molecular Formula:C₄₅H₄₆N₆O₈
Molecular Weight:798.896
Hs Code.:

Synonyms:2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate

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Chemical Property of 2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate

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Technology Process of 2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate

There total 4 articles about 2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1327188-17-9
2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}-4-hydroxybut-2-enoate

: 1327188-12-4
2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate

Guidance literature:: With 2-iodoxybenzoic acid immobilized on polystyrene; In dichloromethane; at 20 ℃; for 0.333333h;
DOI:10.1039/c1ob05320e

Reference yield:

: C₃₂H₄₀N₂O₄Si

: 1327188-12-4
2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 20 °C

2: triethylamine; HATU / N,N-dimethyl-formamide / 20 °C

3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 20 °C

4: 2-iodoxybenzoic acid immobilized on polystyrene / dichloromethane / 0.33 h / 20 °C

With tetrabutyl ammonium fluoride; acetic acid; triethylamine; HATU; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05320e

Reference yield:

: 1327188-16-8
2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-tert-butyldiphenylsilanylhydroxy-2-(6-aminostyryl)but-2-enoate

: 1327188-12-4
2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-oxo-2-{6-[7-(diethylamino)coumarin-3-carboxamide]styryl}but-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; HATU / N,N-dimethyl-formamide / 20 °C

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 20 °C

3: 2-iodoxybenzoic acid immobilized on polystyrene / dichloromethane / 0.33 h / 20 °C

With tetrabutyl ammonium fluoride; acetic acid; triethylamine; HATU; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05320e