2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate

Base Information

Chemical Name:2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate
CAS No.:1047643-29-7
Molecular Formula:C₄₂H₅₆N₂O₈Si
Molecular Weight:745.001
Hs Code.:

Synonyms:2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate

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Chemical Property of 2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate

Chemical Property:

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Technology Process of 2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate

There total 1 articles about 2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1047643-18-4
(E)-tert-butyl 4-(2-(tri-n-butylstannyl)vinyl)phenylcarbamate

: 1047643-25-3
2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (Z)-2-bromo-4-(tert-butyldiphenylsilanyloxy)-2-butenoate

: 1047643-29-7
2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate

Guidance literature:: With lithium chloride; trifuran-2-yl-phosphane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 20 - 115 ℃;

Reference yield:

: 1047643-29-7
2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate

: C₃₂H₄₀N₂O₄Si

Guidance literature:: 2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate; With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.333333h;

With sodium hydroxide; In dichloromethane; water;

Reference yield:

: 1047643-29-7
2-(2-N-tert-butoxycarbonylaminoethoxy)ethyl (E,E)-4-(tert-butyldiphenylsilanyloxy)-2-(4-N-tert-butoxycarbonylaminostyryl)but-2-enoate

: 1327188-16-8
2-{2-{4-[4-(dimethylamino)phenylazo]benzoyl}aminoethoxy}ethyl (E,E)-4-tert-butyldiphenylsilanylhydroxy-2-(6-aminostyryl)but-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 0.33 h / 0 °C

2: dichloromethane / 20 °C

With trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c1ob05320e