methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate

Base Information

Chemical Name:methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate
CAS No.:1020210-48-3
Molecular Formula:C₂₂H₂₂N₄O₂
Molecular Weight:374.442
Hs Code.:

Synonyms:methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate

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Chemical Property of methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate

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Technology Process of methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate

There total 7 articles about methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1020210-41-6
methyl 3-amino-4-[(5-tert-butyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate

: 707-07-3
orthobenzoic acid trimethyl ester

: 1020210-48-3
methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate

Guidance literature:: In N,N-dimethyl-formamide; for 5h; Heating;
DOI:10.1055/s-2008-1032030

Reference yield:

: 82560-12-1,1237537-54-0
3-tert-butyl-1H-pyrazole-5-amine

: 1020210-48-3
methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 2 h / 20 °C

2: hydrazine hydrate / methanol / 1 h / Reflux

3: 140 °C / Neat (no solvent)

With hydrazine hydrate; In methanol; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2011.06.006

Reference yield:

: 1020210-39-2,1304789-08-9
methyl 4-[(3-tert-butyl-1H-pyrazol-5-yl)amino]-3-nitrobenzoate

: 1020210-48-3
methyl 1-(5-tert-butyl-1H-pyrazol-3-yl)-2-phenyl-1H-benzo[d]imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 1 h / Reflux

2: 140 °C / Neat (no solvent)

With hydrazine hydrate; In methanol;
DOI:10.1016/j.ejmech.2011.06.006