(R)-N-Butylidene-1-phenyl-2-methoxyethanamine

Base Information

Chemical Name:(R)-N-Butylidene-1-phenyl-2-methoxyethanamine
CAS No.:252334-54-6
Molecular Formula:C₁₃H₁₉NO
Molecular Weight:205.3
Hs Code.:
DSSTox Substance ID:DTXSID501194619
Nikkaji Number:J1.822.766E

Synonyms:DTXSID501194619;(R)-N-Butylidene-1-phenyl-2-methoxyethanamine;[N(E),alphaR]-N-Butylidene-alpha-(methoxymethyl)benzenemethanamine;252334-54-6

Suppliers and Price of (R)-N-Butylidene-1-phenyl-2-methoxyethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of (R)-N-Butylidene-1-phenyl-2-methoxyethanamine

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:205.146664230
Heavy Atom Count:15
Complexity:173

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCC=NC(COC)C1=CC=CC=C1
Isomeric SMILES:CCCC=N[C@@H](COC)C1=CC=CC=C1

Technology Process of (R)-N-Butylidene-1-phenyl-2-methoxyethanamine

There total 1 articles about (R)-N-Butylidene-1-phenyl-2-methoxyethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64715-85-1,91298-74-7,127180-88-5
(R)-2-methoxy-1-phenylethylamine

: 123-72-8
butyraldehyde

: 252334-54-6
(R)-(E)-N-Butylidene-2-methoxy-1-phenylethylamine

Guidance literature:: With 3 A molecular sieve; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/a905061b

Reference yield: 85.0%

: 1119-51-3
bromopentene

: 252334-54-6
(R)-(E)-N-Butylidene-2-methoxy-1-phenylethylamine

: 252334-55-7
(6S,1'R)-6-(2'-Methoxy-1'-phenylethylamino)non-1-ene

Guidance literature:: bromopentene; With magnesium;

With cerium(III) chloride; In tetrahydrofuran; at 0 ℃; for 1.5h;

(R)-(E)-N-Butylidene-2-methoxy-1-phenylethylamine; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1039/a905061b

Reference yield:

: 252334-54-6
(R)-(E)-N-Butylidene-2-methoxy-1-phenylethylamine

: 252334-56-8
(6S,1'R)-6-(2'-Methoxy-1'-phenylethylamino)nonan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg

1.2: CeCl₃ / tetrahydrofuran / 1.5 h / 0 °C

1.3: 85 percent / tetrahydrofuran / 20 h / 20 °C

2.1: 74 percent / O₂; CuCl₂ / PdCl₂(MeCN)2 / methanol / 2 h / 20 °C

With oxygen; magnesium; copper dichloride; dichloro bis(acetonitrile) palladium(II); In methanol; 1.1: Metallation / 1.2: Metallation / 1.3: Condensation / 2.1: Oxidation;
DOI:10.1039/a905061b