C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾
CAS No.:1620070-38-3
Molecular Formula:C₃₂H₂₃N₂O₄S*Na
Molecular Weight:554.601
Hs Code.:

C<sub>32</sub>H<sub>23</sub>N<sub>2</sub>O<sub>4</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

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Chemical Property of C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

There total 8 articles about C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620070-37-2
C₃₂H₂₄N₂O₄S

: 1620070-38-3
C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: With sodium hydroxide; In methanol; water; at 0 ℃; for 0.5h;

Reference yield:

: 52505-45-0
2-mercaptopyridine-3-carbonitrile

: 1620070-38-3
C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium methylate / N,N-dimethyl-formamide / 0 - 20 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

4.1: triethylamine; dmap / 1,2-dichloro-ethane / 0.25 h / 0 °C

4.2: 0.17 h / 0 °C

4.3: 2 h / 20 °C / Inert atmosphere

5.1: lithium hydroxide monohydrate / 20 °C

6.1: sodium hydroxide / methanol; water / 0.5 h / 0 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium hydroxide monohydrate; sodium methylate; potassium carbonate; triethylamine; sodium hydroxide; In methanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 6602-54-6
2-chloro-3-pyridinecarbonitrile

: 1620070-38-3
C₃₂H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium methylate / N,N-dimethyl-formamide / 24 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / Reflux

3.1: sodium methylate / N,N-dimethyl-formamide / 0 - 20 °C

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

6.1: triethylamine; dmap / 1,2-dichloro-ethane / 0.25 h / 0 °C

6.2: 0.17 h / 0 °C

6.3: 2 h / 20 °C / Inert atmosphere

7.1: lithium hydroxide monohydrate / 20 °C

8.1: sodium hydroxide / methanol; water / 0.5 h / 0 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium hydroxide monohydrate; sodium methylate; sodium hydride; potassium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;