ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

Base Information

Chemical Name:ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate
CAS No.:129813-55-4
Molecular Formula:C₂₂H₂₇NO₄
Molecular Weight:369.461
Hs Code.:

Synonyms:ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

Suppliers and Price of ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

There total 1 articles about ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3699-66-9
ethyl 2-diethoxyphosphorylpropionate

: 129813-53-2
3-(4-formyl-2,5-dimethoxy-3,6-dimethylbenzyl)pyridine

: 129813-55-4
ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 0 deg C, 20 min, 2.) RT, 1 h;
DOI:10.1021/jm00105a042

Reference yield:

: 129813-55-4
ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

: (E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid ethyl ester

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; at 0 ℃; for 1h;
DOI:10.1021/jm00105a042

Reference yield:

: 129813-55-4
ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

: 129813-32-7
(E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: cerium ammonium nitrate (CAN) / H₂O; acetonitrile / 1 h / 0 °C

2: 70 percent / concd. aq. HCl / 2 h / Heating

With hydrogenchloride; ammonium cerium(IV) nitrate; In water; acetonitrile;
DOI:10.1021/jm00105a042