2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester

Base Information

Chemical Name:2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester
CAS No.:104484-34-6
Molecular Formula:C₁₆H₁₈O₆S
Molecular Weight:338.381
Hs Code.:

Synonyms:2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester

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Chemical Property of 2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester

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Technology Process of 2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester

There total 1 articles about 2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 93515-30-1,5740-35-2
3-(4-methoxyphenyl)-2-sulfanylpropenoic acid

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 104484-34-6
2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 1h; Heating;

Reference yield: 81.0%

: 104484-34-6
2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester

: 104484-21-1
5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-2-methyl-6-oxo-5,6-dihydro-[1,4]oxathiine-3-carboxylic acid ethyl ester

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; benzene; for 1h; Ambient temperature;

Reference yield:

: 104484-34-6
2-[(E)-1-Carboxy-2-(4-methoxy-phenyl)-vinylsulfanyl]-3-oxo-butyric acid ethyl ester

: 104484-41-5
5-[1-(4-Methoxy-phenyl)-meth-(Z)-ylidene]-2-methyl-4,6-dioxo-5,6-dihydro-4H-4λ⁴-[1,4]oxathiine-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / SOCl₂ / dimethylformamide; benzene / 1 h / Ambient temperature

2: 61 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 2 h / 0 - 5 °C

With thionyl chloride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; benzene;