tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate

Base Information

Chemical Name:tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate
CAS No.:308846-62-0
Molecular Formula:C₁₈H₂₃FN₂O₄
Molecular Weight:350.39
Hs Code.:

Synonyms:tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate

Chemical Property:

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Technology Process of tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate

There total 5 articles about tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51779-32-9
iminodicarboxylic acid di-tert-butyl ester

: 222978-03-2
4-cyano-3-fluorobenzylbromide

: 308846-62-0
tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1021/jm030025j

Reference yield:

: 85070-67-3
2-fluoro-4-methylbenzonitrile

: 308846-62-0
tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate

Guidance literature:: Multi-step reaction with 2 steps

1: NBS / CCl₄ / Heating

2: NaH / tetrahydrofuran

With N-Bromosuccinimide; sodium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/j.bmcl.2007.05.090

Reference yield:

: 452-74-4
4-bromo-3-fluorotoluene

: 308846-62-0
tert-butyl {(tert-butoxy)-N-[(4-cyano-3-fluorophenyl)methyl]carbonylamino}formate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / Heating

2: N-bromosuccinimide; benzoyl peroxide / CCl₄ / Heating

3: NaH / tetrahydrofuran

With N-Bromosuccinimide; sodium hydride; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm030025j