5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide

Base Information

Chemical Name:5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide
CAS No.:1403473-14-2
Molecular Formula:C₂₀H₁₄Cl₂N₄O₄
Molecular Weight:445.262
Hs Code.:

Synonyms:5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide

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Chemical Property of 5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide

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Technology Process of 5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide

There total 5 articles about 5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1403473-44-8
5-(3,5-dichlorophenyl)-N-(2,4-dioxoimidazolidin-1-yl)-2-furamide

: 6959-48-4
3-chloromethylpyridinium chloride

: 1403473-14-2
5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide

Guidance literature:: 5-(3,5-dichlorophenyl)-N-(2,4-dioxoimidazolidin-1-yl)-2-furamide; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.166667h;

3-chloromethylpyridinium chloride; In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1016/j.bmc.2012.08.062

Reference yield:

: 98-01-1
furfural

: 1403473-14-2
5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium nitrite; hydrogenchloride / water / 0.33 h / 0 - 110 °C

1.2: 0.25 h / 0 °C

1.3: 14 h / 0 - 20 °C

2.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / water; tert-butyl alcohol / 11 h / 20 °C

3.1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; 4-methyl-morpholine / water; methanol / 19 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

4.2: 6 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; sodium nitrite; In methanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: |Meerwein Arylation / 1.2: |Meerwein Arylation / 1.3: |Meerwein Arylation;
DOI:10.1016/j.bmc.2012.08.062

Reference yield:

: 106827-27-4
5-(3,5-dichlorophenyl)furan-2-carbaldehyde

: 1403473-14-2
5-(3,5-dichlorophenyl)-N-{2,4-dioxo-3-[(pyridin-3-yl)methyl]imidazolidin-1-yl}-2-furamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / water; tert-butyl alcohol / 11 h / 20 °C

2.1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; 4-methyl-morpholine / water; methanol / 19 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

3.2: 6 h / 20 °C

With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In methanol; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmc.2012.08.062