tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate

Base Information

Chemical Name:tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate
CAS No.:1361185-23-0
Molecular Formula:C₁₇H₂₄O₄
Molecular Weight:292.375
Hs Code.:

Synonyms:tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate

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Chemical Property of tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate

Chemical Property:

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Technology Process of tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate

There total 3 articles about tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1361185-24-1
4-bromo-1-[(methoxymethoxy)methyl]-2-methylbenzene

: 1361185-23-0
tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 140 ℃; for 2h; Inert atmosphere;

Reference yield:

: 68837-59-2
4-bromo-2-methylbenzoic acid

: 1361185-23-0
tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: borane-THF / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / Reflux

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 2 h / 140 °C / Inert atmosphere

With borane-THF; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;

Reference yield:

: 17100-58-2
4-bromo-2-methylbenzyl alcohol

: 1361185-23-0
tert-butyl (2E)-3-{4-[(methoxymethoxy)methyl]-3-methylphenyl}prop-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 2 h / 140 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane;