(E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide

Base Information

Chemical Name:(E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide
CAS No.:1416978-69-2
Molecular Formula:C₂₀H₁₆Cl₃F₃N₂O
Molecular Weight:463.714
Hs Code.:

Synonyms:(E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide

Chemical Property:

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Technology Process of (E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide

There total 6 articles about (E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1416980-59-0
(E)-(4-(4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)hydrazine

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 1416978-69-2
(E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide

Guidance literature:: With SiO₂; In dichloromethane; ethyl acetate; Petroleum ether;

Reference yield:

: 184474-85-9
2-((4-Bromophenyl)amino)isoindoline-1,3-dione

: 1416978-69-2
(E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: SiO₂ / water; Petroleum ether; ethyl acetate; 1,2-dimethoxyethane

2: SiO₂ / 1,2-dichloro-benzene; Petroleum ether; ethyl acetate

3: hydrazine hydrate / ethanol

4: SiO₂ / dichloromethane; Petroleum ether; ethyl acetate

With hydrazine hydrate; SiO₂; In 1,2-dimethoxyethane; ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-benzene; Petroleum ether;

Reference yield:

: 622-88-8,41931-18-4
4-bromophenylhydrazine hydrochloride

: 1416978-69-2
(E)-N'-(4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)cyclopropanecarbohydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: SiO₂ / Petroleum ether; ethyl acetate

2: SiO₂ / water; Petroleum ether; ethyl acetate; 1,2-dimethoxyethane

3: SiO₂ / 1,2-dichloro-benzene; Petroleum ether; ethyl acetate

4: hydrazine hydrate / ethanol

5: SiO₂ / dichloromethane; Petroleum ether; ethyl acetate

With hydrazine hydrate; SiO₂; In 1,2-dimethoxyethane; ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-benzene; Petroleum ether;