(E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione

Base Information

Chemical Name:(E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione
CAS No.:1416980-58-9
Molecular Formula:C₂₄H₁₄Cl₃F₃N₂O₂
Molecular Weight:525.742
Hs Code.:

Synonyms:(E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione

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Chemical Property of (E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione

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Technology Process of (E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione

There total 5 articles about (E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1416979-50-4
5-(1-bromo-2,2,2-trifluoroethyl)-1,2,3-trichlorobenzene

: 1416980-57-8
2-((4-Vinylphenyl)amino)isoindoline-1,3-dione

: 1416980-58-9
(E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione

Guidance literature:: [2,2]bipyridinyl; copper(l) chloride; In 1,2-dichloro-benzene; at 180 ℃; for 2h; Inert atmosphere;

Reference yield: 75.0%

: 366-18-7
[2,2]bipyridinyl

: 1416979-50-4
5-(1-bromo-2,2,2-trifluoroethyl)-1,2,3-trichlorobenzene

: 1416980-57-8
2-((4-Vinylphenyl)amino)isoindoline-1,3-dione

: 1416980-58-9
(E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione

Guidance literature:: With SiO₂; In ethyl acetate; 1,2-dichloro-benzene; Petroleum ether;

Reference yield:

: 85-44-9
phthalic anhydride

: 1416980-58-9
(E)-2-((4-(4,4,4-Trifluoro-3-(3,4,5-trichlorophenyl)but-1-en-1-yl)phenyl)amino)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 1 h / 130 °C / Inert atmosphere

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 0.5 h / 150 °C / Microwave irradiation

3: [2,2]bipyridinyl; copper(l) chloride / 1,2-dichloro-benzene / 2 h / 180 °C / Inert atmosphere

With potassium carbonate; acetic acid; [2,2]bipyridinyl; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) chloride; In 1,2-dimethoxyethane; water; 1,2-dichloro-benzene;