C₄₇H₆₈O₁₀Si₂

Base Information

Chemical Name:C₄₇H₆₈O₁₀Si₂
CAS No.:791072-86-1
Molecular Formula:C₄₇H₆₈O₁₀Si₂
Molecular Weight:849.222
Hs Code.:

C<sub>47</sub>H<sub>68</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₇H₆₈O₁₀Si₂

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Chemical Property of C₄₇H₆₈O₁₀Si₂

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Technology Process of C₄₇H₆₈O₁₀Si₂

There total 10 articles about C₄₇H₆₈O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 791072-95-2
2,2-Dimethyl-propionic acid (2S,3R)-3-formyl-2-(4-methoxy-benzyloxy)-5-[(3S,5R)-3-methoxymethoxy-5-((R)-1-phenoxy-prop-2-ynyl)-5-triethylsilanyloxy-cyclopent-1-enyl]-3-triethylsilanyloxy-pent-4-ynyl ester

: 791072-86-1
C₄₇H₆₈O₁₀Si₂

Guidance literature:: With n-butyllithium; cerium(III) chloride; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; hexane; at -25 - 0 ℃;
DOI:10.1021/ol048494i

Reference yield:

: 994-30-9
triethylsilyl chloride

: 791072-86-1
C₄₇H₆₈O₁₀Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: imidazole / dimethylformamide / 1.17 h / 50 °C

2: 1.45 g / HN(TMS)2; n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

3: iPr₂NEt; CuI / Pd₂(dba)3*CHCl₃ / dimethylformamide / 1 h / 20 °C

4: 1.79 g / TBAF / tetrahydrofuran / 1 h / -60 °C

5: 88 percent / ZnBr₂ / CH₂Cl₂ / 2.5 h / 20 °C

6: 71 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

7: 98 percent / CeCl₃; n-BuLi; HN(TMS)2 / tetrahydrofuran; hexane / -25 - 0 °C

With 1H-imidazole; copper(l) iodide; n-butyllithium; cerium(III) chloride; tetrabutyl ammonium fluoride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 1,1,1,3,3,3-hexamethyl-disilazane; zinc dibromide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 3: Sonogashira coupling / 6: Dess-Martin oxidation;
DOI:10.1021/ol048494i

Reference yield:

: 791072-89-4
(2S,3S,6S)-2-Ethynyl-4-iodo-6-methoxymethoxy-1-oxa-spiro[2.4]hept-4-ene

: 791072-86-1
C₄₇H₆₈O₁₀Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 83 percent / CsF / dimethylformamide / 4 h / 80 °C

2: imidazole / dimethylformamide / 1.17 h / 50 °C

3: 1.45 g / HN(TMS)2; n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

4: iPr₂NEt; CuI / Pd₂(dba)3*CHCl₃ / dimethylformamide / 1 h / 20 °C

5: 1.79 g / TBAF / tetrahydrofuran / 1 h / -60 °C

6: 88 percent / ZnBr₂ / CH₂Cl₂ / 2.5 h / 20 °C

7: 71 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

8: 98 percent / CeCl₃; n-BuLi; HN(TMS)2 / tetrahydrofuran; hexane / -25 - 0 °C

With 1H-imidazole; copper(l) iodide; n-butyllithium; cerium(III) chloride; tetrabutyl ammonium fluoride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; cesium fluoride; 1,1,1,3,3,3-hexamethyl-disilazane; zinc dibromide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 4: Sonogashira coupling / 7: Dess-Martin oxidation;
DOI:10.1021/ol048494i