methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

Base Information

• Chemical Name: methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside
• CAS No.: 866885-23-6
• Molecular Formula: C₃₇H₄₄O₈Si
• Molecular Weight: 644.837

Synonyms:methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

Chemical Property of methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

There total 18 articles about methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl 3,4-di-O-benzyl-2-O-levulinoyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside (866885-24-7) → methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside (866885-23-6)

Guidance literature:

With hydrazinium monoacetate; In methanol; dichloromethane; at 20 ℃; for 1.5h;

DOI:10.1081/CAR-200067008

Reference yield: 95.0%

methyl 3,4-di-O-benzyl-2-O-(9-fluorenylmethoxycarbonyl)-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside (866885-28-1) → methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside (866885-23-6)

Guidance literature:

With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

DOI:10.1081/CAR-200067008

Reference yield: 83.0%

methyl 2-O-allyl-3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside (866885-29-2) → methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside (866885-23-6)

Guidance literature:

With sodium acetate; acetic acid; palladium dichloride; In water; at 80 ℃; for 0.666667h;

DOI:10.1081/CAR-200067008

upstream raw materials:

methyl 2-O-allyl-3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

methyl 3,4-di-O-benzyl-2-O-levulinoyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

methyl 3,4-di-O-benzyl-2-O-para-methoxybenzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

methyl 3,4-di-O-benzyl-2-O-(9-fluorenylmethoxycarbonyl)-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

Downstream raw materials:

methyl 2-O-allyl-3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

methyl 3,4-di-O-benzyl-2-O-(9-fluorenylmethoxycarbonyl)-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

methyl 3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-2-O-pivaloyl-β-D-glucopyranoside

methyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-{2-[dimethyl(2-naphthylmethyl)silyl]ethoxycarbonyl}-β-D-glucopyranoside

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