S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate

Base Information

Chemical Name:S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate
CAS No.:1370229-42-7
Molecular Formula:C₁₅H₁₉IN₂O₃S₃
Molecular Weight:498.43
Hs Code.:

Synonyms:S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate

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Chemical Property of S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate

Chemical Property:

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Technology Process of S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate

There total 3 articles about S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 59463-54-6
S-cyanomethyl O-ethyl carbonodithioate

: 143937-64-8
N-allyl-N-(4-iodophenyl)methanesulfonamide

: 1370229-42-7
S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; for 2.5h; Inert atmosphere; Reflux;
DOI:10.1021/ol3005276

Reference yield:

: 102294-59-7
N-(4-iodophenyl)-methanesulfonamide

: 1370229-42-7
S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Inert atmosphere; Cooling with ice

1.2: 2 h / Inert atmosphere

2.1: dilauryl peroxide / ethyl acetate / 2.5 h / Inert atmosphere; Reflux

With dilauryl peroxide; sodium hydride; In ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol3005276

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1370229-42-7
S-1-(4-iodophenylmethanesulfonylamino)-4-cyanobutan-2-yl O-ethyl carbonodithioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 1,2-dichloro-ethane / 2 - 3 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Inert atmosphere; Cooling with ice

2.2: 2 h / Inert atmosphere

3.1: dilauryl peroxide / ethyl acetate / 2.5 h / Inert atmosphere; Reflux

With pyridine; dilauryl peroxide; sodium hydride; In ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol3005276