1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Base Information

• Chemical Name: 1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
• CAS No.: 1073542-79-6
• Molecular Formula: C₂₆H₂₆N₂O
• Molecular Weight: 382.505

Synonyms:1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Chemical Property of 1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Chemical Property:

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Technology Process of 1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

There total 1 articles about 1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-Benzyloxybenzaldehyde (1700-37-4) + 2-(5-ethyl-1H-indol-3-yl)ethylamine (62500-88-3) → 1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole (1073542-79-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2008.07.056

Reference yield: 75.0%

1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole (1073542-79-6) → 5-ethyl-2-(3-hydroxybenzyl)tryptamine hydrochloride

Guidance literature:

1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole; With 10% Pd/C; hydrogen; In methanol; at 20 ℃; for 3h; under 760.051 Torr;

With hydrogenchloride; In diethyl ether; ethyl acetate;

DOI:10.1016/j.tet.2008.07.056

Reference yield: 65.0%

1-(3-benzyloxyphenyl)-6-ethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole (1073542-79-6) + 1-iodo-propane (107-08-4) → 6-ethyl-1-(3-benzyloxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole (1073542-83-2)

Guidance literature:

With potassium carbonate; In acetonitrile; for 24h; Reflux;

DOI:10.1016/j.tet.2008.07.056

upstream raw materials:

3-Benzyloxybenzaldehyde

2-(5-ethyl-1H-indol-3-yl)ethylamine

Downstream raw materials:

6-ethyl-1-(3-benzyloxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

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