dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester

Base Information

Chemical Name:dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester
CAS No.:899794-60-6
Molecular Formula:C₂₆H₂₄O₃S₂
Molecular Weight:448.607
Hs Code.:

Synonyms:dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester

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Chemical Property of dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester

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Technology Process of dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester

There total 5 articles about dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 899794-51-5
dithiocarbonic acid S-[4-(biphenyl-4-yl)-4-oxo-1-(2-phenyl[1,3]dioxolan-2-yl)butyl] ester O-ethyl ester

: 899794-60-6
dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1055/s-2006-926464

Reference yield:

: 29568-66-9
2-phenyl-2-vinyl-[1,3]dioxolane

: 899794-60-6
dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / 2,6-lutidine; dilauroyl peroxide / cyclohexane / Heating

2: 83 percent / aq. trifluoroacetic acid / CH₂Cl₂ / 4 h / 20 °C

With 2,6-dimethylpyridine; dilauryl peroxide; trifluoroacetic acid; In dichloromethane; cyclohexane;
DOI:10.1055/s-2006-926464

Reference yield:

: 936-59-4
3-chloropropiophenone

: 899794-60-6
dithiocarbonic acid S-[1-benzoyl-4-(biphenyl-4-yl)-4-oxobutyl] ester O-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 54 percent / ethanol / 4 h / Heating

2: 54 percent / p-TsOH / toluene / 8 h / Heating

3: 54 percent / dimethylethylene urea; t-BuOK / toluene / Heating

4: 71 percent / 2,6-lutidine; dilauroyl peroxide / cyclohexane / Heating

5: 83 percent / aq. trifluoroacetic acid / CH₂Cl₂ / 4 h / 20 °C

With 2,6-dimethylpyridine; dimethyl-ethylene urea; dilauryl peroxide; potassium tert-butylate; toluene-4-sulfonic acid; trifluoroacetic acid; In ethanol; dichloromethane; cyclohexane; toluene;
DOI:10.1055/s-2006-926464