6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide

Base Information

Chemical Name:6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide
CAS No.:1233979-41-3
Molecular Formula:C₃₂H₃₂N₂O₆
Molecular Weight:540.616
Hs Code.:

Synonyms:6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide

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Chemical Property of 6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide

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Technology Process of 6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide

There total 6 articles about 6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1233979-39-9
3-(benzyloxy)-2-bromo-4-methoxy-N-methylbenzamide

: 1233979-41-3
6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide

Guidance literature:: With copper; In N,N-dimethyl-formamide; for 4h; Inert atmosphere; Reflux;
DOI:10.2174/157340611796150914

Reference yield:

: 1233979-40-2
C₁₅H₁₂BrClO₃

: 1233979-41-3
6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; dichloromethane; water / 2 h / 20 °C / Cooling with ice

2: copper / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux

With copper; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 2: Ullmann condensation;
DOI:10.2174/157340611796150914

Reference yield:

: 135586-17-3
3-(benzyloxy)-2-bromo-4-methoxybenzoic acid

: 1233979-41-3
6,6'-bis(benzyloxy)-5,5'-dimethoxy-N,N'-dimethylbiphenyl-2,2'-dicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

2: tetrahydrofuran; dichloromethane; water / 2 h / 20 °C / Cooling with ice

3: copper / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux

With thionyl chloride; copper; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 3: Ullmann condensation;
DOI:10.2174/157340611796150914