(4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine

Base Information

Chemical Name:(4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine
CAS No.:163625-45-4
Molecular Formula:C₂₃H₃₄N₂O₆
Molecular Weight:434.533
Hs Code.:

Synonyms:(4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine

There total 4 articles about (4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 77-76-9
2,2-dimethoxy-propane

: 163625-40-9
(2S,3R)-(E)-N^α-(tert-Butoxycarbonyl)-N-methoxy-N-methyl-2-amino-6-(benzyloxy)-3-hydroxy-4-hexenamide

: 163625-45-4
(4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.1021/jo00111a034

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 163625-45-4
(4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) r.t., overnight

2: 79 percent / p-TsOH*H₂O / benzene / Heating

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo00111a034

Reference yield:

: 1026840-32-3
(E)-(2S,3R)-2-Amino-6-benzyloxy-3-hydroxy-hex-4-enoic acid methoxy-methyl-amide

: 163625-45-4
(4S,5R)-5-<(E)-3-(Benzyloxy)-1-propenyl>-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-(N-methoxy-N-methylcarbamoyl)oxazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) r.t., overnight

2: 79 percent / p-TsOH*H₂O / benzene / Heating

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo00111a034