Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester

Base Information

Chemical Name:Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester
CAS No.:867266-54-4
Molecular Formula:C₃₂H₄₉NO₆Si
Molecular Weight:571.83
Hs Code.:

Synonyms:Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester

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Chemical Property of Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester

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Technology Process of Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester

There total 3 articles about Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 867266-53-3
((1S,2S)-2-Benzyloxy-1-hydroxymethyl-3-triisopropylsilanyloxy-propyl)-carbamic acid tert-butyl ester

: 98-88-4
benzoyl chloride

: 867266-54-4
Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1055/s-2005-871954

Reference yield:

: 867266-52-2
[2-benzyloxy-1-(tert-butyl-dimethyl-silanyloxymethyl)-3-triisopropylsilanyloxy-propyl]-carbamic acid tert-butyl ester

: 867266-54-4
Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / PPTS / tetrahydrofuran; ethanol / 120 h

2: 98 percent / pyridine / 12 h / 20 °C

With pyridine; pyridinium p-toluenesulfonate; In tetrahydrofuran; ethanol;
DOI:10.1055/s-2005-871954

Reference yield:

: 867266-55-5
[(1S,2S)-2-Benzyloxy-1-(4-methoxy-phenoxymethyl)-3-triisopropylsilanyloxy-propyl]-carbamic acid tert-butyl ester

: 867266-54-4
Benzoic acid (2S,3S)-3-benzyloxy-2-tert-butoxycarbonylamino-4-triisopropylsilanyloxy-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. CAN / acetonitrile / 0.17 h / 0 °C

2: 98 percent / pyridine / 12 h / 20 °C

With pyridine; ammonium cerium(IV) nitrate; In acetonitrile;
DOI:10.1055/s-2005-871954