3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester

Base Information

Chemical Name:3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester
CAS No.:120385-97-9
Molecular Formula:C₂₈H₂₈ClN₃O₆S₂
Molecular Weight:602.132
Hs Code.:

3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester

Synonyms:3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester

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Chemical Property of 3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester

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Technology Process of 3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester

There total 2 articles about 3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 683-57-8
bromo-acetic acid amide

: 120386-00-7
5-(3-(2-(7-CHLOROQUINOLIN-2-YL)ETHENYL)PHENYL)-4,6-DITHIANONANEDIOIC ACID

: 120385-97-9
3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 18h; Ambient temperature;
DOI:10.1021/jo00313a010

Reference yield:

: 120385-96-8
dimethyl 5-<3-<2-(7-chloro-2-quinolinyl)-(E)-ethenyl>phenyl>-4,6-dithianonanedioate

: 120385-97-9
3-((2-Carbamoylmethoxycarbonyl-ethylsulfanyl)-{3-[(E)-2-(7-chloro-quinolin-2-yl)-vinyl]-phenyl}-methylsulfanyl)-propionic acid carbamoylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1 percent / H₂O / 336 h / 37 °C / Pseudomonas sp. lipase, Triton X-100, Na₂PO₄, H₃PO₄, pH 7.5; enantioselectivity; other enzymes, other surfactants, other solvents, other diesters

2: 77 percent / diisopropylethylamine / dimethylformamide / 18 h / Ambient temperature

With N-ethyl-N,N-diisopropylamine; In water; N,N-dimethyl-formamide;
DOI:10.1021/jo00313a010