(S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate

Base Information

Chemical Name:(S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate
CAS No.:1192262-08-0
Molecular Formula:C₂₃H₂₈INO₆
Molecular Weight:541.383
Hs Code.:

Synonyms:(S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate

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Technology Process of (S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate

There total 1 articles about (S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 107-30-2
chloromethyl methyl ether

: 268741-98-6
(2S)-2-tert-butoxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid benzyl ester

: 1192262-08-0
(S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 18h;
DOI:10.1021/jo901744y

Reference yield:

: 1192262-14-8
Bn-MeHis-OAllyl

: 1192262-08-0
(S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate

: 1192262-21-7
(S)-allyl 2-(benzyl(methyl)amino)-3-(1-(5-((S)-3-(benzyloxy)-2-(tert-butoxycarbonylamino)-3-oxopropyl)-2-(methoxymethoxy)phenyl)-1H-imidazol-4-yl)propanoate

Guidance literature:: (S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate; With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; bis(tri-n-butyltin); In 1-methyl-pyrrolidin-2-one;

With lead(IV) tetraacetate; mercury(II) trifluoroacetate; sodium hydroxide; In chloroform; water; at 30 ℃; Darkness; Inert atmosphere;

Bn-MeHis-OAllyl; With copper diacetate; In dichloromethane; at 20 ℃; for 4h; regioselective reaction;
DOI:10.1021/jo901744y

Reference yield:

: 866392-18-9
(S)-methyl 2-(benzyl(methyl)amino)-3-(1H-imidazol-4-yl)propanoate

: 1192262-08-0
(S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate

: 1192262-19-3
(S)-benzyl 3-(3-(4-((S)-2-(benzyl(methyl)amino)-3-methoxy-3-oxopropyl)-1H-imidazol-1-yl)-4-(methoxymethoxy)phenyl)-2-(tert-butoxycarbonylamino)propanoate

Guidance literature:: (S)-benzyl 2-(tert-butoxycarbonylamino)-3-(3-iodo-4-(methoxymethoxy)phenyl)propanoate; With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; bis(tri-n-butyltin); In 1-methyl-pyrrolidin-2-one;

With lead(IV) tetraacetate; mercury(II) trifluoroacetate; sodium hydroxide; In chloroform; water; at 30 ℃; Darkness; Inert atmosphere;

(S)-methyl 2-(benzyl(methyl)amino)-3-(1H-imidazol-4-yl)propanoate; With copper diacetate; In dichloromethane; at 20 ℃; for 4h; regioselective reaction;
DOI:10.1021/jo901744y