4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt

Base Information

Chemical Name:4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt
CAS No.:1446443-91-9
Molecular Formula:C₄H₁₁N*C₁₅H₁₂ClF₃N₂O₄S
Molecular Weight:481.924
Hs Code.:

Synonyms:4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt

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Chemical Property of 4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt

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Technology Process of 4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt

There total 4 articles about 4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354960-58-9
4-[4-chloro-3-(trifluoromethyl)phenoxy]benzoic acid

: 15211-35-5
N-(4-methoxybenzyl)-N-methylsulfamide

: 109-89-7
diethylamine

: 1446443-91-9
4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt

Guidance literature:: 4-[4-chloro-3-(trifluoromethyl)phenoxy]benzoic acid; N-(4-methoxybenzyl)-N-methylsulfamide; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 16h;

With trifluoroacetic acid; In dichloromethane; for 8h;

diethylamine; In water; acetonitrile;

Reference yield:

: 37900-81-5
2-chloro-4-hydroxybenzotrifluoride

: 1446443-91-9
4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dimethyl sulfoxide / 48 h / 110 °C

2.1: water; potassium hydroxide / ethanol / 16 h / Inert atmosphere; Reflux

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

3.2: 8 h

With dmap; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In ethanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1194-02-1,143234-87-1
4-fluorobenzonitrile

: 1446443-91-9
4-[4-chloro-3-(trifluoromethyl)phenoxy]-N-[(methylamino)sulfonyl]benzamide diethylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dimethyl sulfoxide / 48 h / 110 °C

2.1: water; potassium hydroxide / ethanol / 16 h / Inert atmosphere; Reflux

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

3.2: 8 h

With dmap; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In ethanol; dichloromethane; dimethyl sulfoxide;