(1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid

Base Information

Chemical Name:(1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid
CAS No.:147201-85-2
Molecular Formula:C₁₉H₂₆N₂O₅
Molecular Weight:362.426
Hs Code.:

Synonyms:(1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid

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Chemical Property of (1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid

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Technology Process of (1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid

There total 3 articles about (1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147148-15-0
(1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid methyl ester

: 147201-85-2
(1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid

Guidance literature:: With sodium hydroxide; In methanol; for 4h;
DOI:10.1021/jm00058a006

Reference yield:

: 88335-91-5
cyclohexane-1,2-dicarboxylic acid monomethyl ester

: 147201-85-2
(1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / oxalyl chloride / benzene / 2 h / Ambient temperature

2: NEt₃ / CH₂Cl₂ / 0 - 5 °C

3: 1 N NaOH / methanol / 4 h

With sodium hydroxide; oxalyl dichloride; triethylamine; In methanol; dichloromethane; benzene;
DOI:10.1021/jm00058a006

Reference yield:

: 147201-81-8
(1R,2S)-cis-2-(methoxycarbonyl)cyclohexanecarbonyl chloride

: 147201-85-2
(1S,2R)-2-[(Benzyloxycarbamoyl-methyl)-ethyl-carbamoyl]-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / CH₂Cl₂ / 0 - 5 °C

2: 1 N NaOH / methanol / 4 h

With sodium hydroxide; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm00058a006