Cyclohexanecarboxylic acid, 2-(chlorocarbonyl)-, methyl ester, (1S-cis)- (9CI)

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 2-(chlorocarbonyl)-, methyl ester, (1S-cis)- (9CI)
CAS No.:147201-81-8
Molecular Formula:C9H13 Cl O3
Molecular Weight:204.653
Hs Code.:
Mol file:147201-81-8.mol

Synonyms:Cyclohexanecarboxylicacid, 2-(chlorocarbonyl)-, methyl ester, (1S-cis)-

Suppliers and Price of Cyclohexanecarboxylic acid, 2-(chlorocarbonyl)-, methyl ester, (1S-cis)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Cyclohexanecarboxylic acid, 2-(chlorocarbonyl)-, methyl ester, (1S-cis)- (9CI)

Chemical Property:

Boiling Point:114.5 - 115 °C (7 mmHg)
PSA：43.37000
LogP:1.73120

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxylic acid, 2-(chlorocarbonyl)-, methyl ester, (1S-cis)- (9CI)

There total 4 articles about Cyclohexanecarboxylic acid, 2-(chlorocarbonyl)-, methyl ester, (1S-cis)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 88335-91-5
cyclohexane-1,2-dicarboxylic acid monomethyl ester

: 147201-81-8
(1R,2S)-cis-2-(methoxycarbonyl)cyclohexanecarbonyl chloride

Guidance literature:: With oxalyl dichloride; In benzene; for 2h; Ambient temperature;
DOI:10.1021/jm00058a006

Reference yield:

: 2484-60-8,2778-62-3,7719-08-6,52782-07-7,88335-91-5,88335-92-6,96894-64-3,111955-05-6
(1S*,2S*)-2-(methoxycarbonyl)cyclohexane-1-carboxylic acid

: 52479-89-7,52841-95-9,71606-03-6,111955-06-7,147201-81-8
(+/-)-trans-2-chlorocarbonyl-cyclohexanecarboxylic acid methyl ester

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 2h;

Reference yield:

: 13149-00-3
1,2-cis-cyclohexanedicarboxylic anhydride

: 147201-81-8
(1R,2S)-cis-2-(methoxycarbonyl)cyclohexanecarbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 4-((4-((1S)-hydroxy((2R,4S,5R)-5-vinylquinuclidin-2-yl)methyl)quinolin-6-yl)oxy)butanoic acid modified Fe₃O₄ nanoparticles / diethyl ether / 60 h / -45 °C / Inert atmosphere

2: thionyl chloride / toluene / 0.17 h / 0 °C

With thionyl chloride; In diethyl ether; toluene;
DOI:10.1039/d1nj04081b