diphenylphosphorylthioformic acid pyrrolidide

Base Information

• Chemical Name: diphenylphosphorylthioformic acid pyrrolidide
• CAS No.: 1021879-90-2
• Molecular Formula: C₁₇H₁₈NOPS
• Molecular Weight: 315.376

Synonyms:diphenylphosphorylthioformic acid pyrrolidide

Chemical Property of diphenylphosphorylthioformic acid pyrrolidide

Chemical Property:

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Technology Process of diphenylphosphorylthioformic acid pyrrolidide

There total 2 articles about diphenylphosphorylthioformic acid pyrrolidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

pyrrolidine (123-75-1) + α-(diphenylphosphoryl)methyl 5-(1-phenyl)-1H-tetrazolyl sulfoxide (1021879-81-1) → phenyl-1H-tetrazole (5378-52-9) + diphenylphosphorylthioformic acid pyrrolidide (1021879-90-2)

Guidance literature:

In 1,4-dioxane; at 90 ℃; for 1h;

DOI:10.1016/j.tet.2008.01.082

Reference yield: 81.0%

pyrrolidine (123-75-1) + α-(diphenylphosphoryl)methyl 2-benzothiazolylsulfoxide (1028454-88-7) → diphenylphosphorylthioformic acid pyrrolidide (1021879-90-2) + α-(diphenylphosphoryl)methyl 2-benzothiazolylsulfide (1028454-86-5) + 2-(pyrrolidin-1-yl)benzo[d]thiazole (19983-29-0)

Guidance literature:

In 1,4-dioxane; at 90 ℃; for 0.5h;

DOI:10.1016/j.tet.2008.02.028

upstream raw materials:

pyrrolidine

α-(diphenylphosphoryl)methyl 5-(1-phenyl)-1H-tetrazolyl sulfoxide

α-(diphenylphosphoryl)methyl 2-benzothiazolylsulfoxide

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