(S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate

Base Information

• Chemical Name: (S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate
• CAS No.: 1206481-38-0
• Molecular Formula: C₃₈H₄₆O₉
• Molecular Weight: 646.778
• Mol file: 1206481-38-0.mol

Synonyms:(S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate

Chemical Property of (S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate

There total 1 articles about (S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-ethenyl-3,4,6-trimethoxybenzoic acid (1206481-37-9) + (R)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-ol (1206481-36-8) → (S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate (1206481-38-0)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In diethyl ether; toluene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.024

Reference yield:

(S)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-yl 3,4,6-trimethoxy-2-vinylbenzoate (1206481-38-0) → C30H38O8 (1206481-52-8)

Guidance literature:

With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 - 20 ℃; pH=7; aq. phosphate buffer; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.024

upstream raw materials:

2-ethenyl-3,4,6-trimethoxybenzoic acid

(R)-5-((2S,4S,5S,6R)-6-allyl-5-(4-methoxybenzyloxy)-2-phenyl-1,3-dioxan-4-yl)pentan-2-ol

Downstream raw materials:

C₃₀H₃₈O₈