2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione

Base Information

Chemical Name:2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione
CAS No.:2222257-79-4
Molecular Formula:C₂₀H₂₀N₂O₆
Molecular Weight:384.389
Hs Code.:

Synonyms:2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione

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Chemical Property of 2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione

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Technology Process of 2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione

There total 16 articles about 2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 2-(3,4-dimethoxyphenyl)-6-methyl-3-oxopyridazine-4-carbonyl chloride

: 504-02-9
1,3-cylohexanedione

: 2222257-79-4
2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione

Guidance literature:: 2-(3,4-dimethoxyphenyl)-6-methyl-3-oxopyridazine-4-carbonyl chloride;

1,3-cylohexanedione; With triethylamine; In dichloromethane; at 0 ℃; for 0.25h;

With triethylamine; 2-hydroxy-2-methylpropanenitrile; In dichloromethane; at 20 - 40 ℃; for 22h;

Reference yield: 30.0%

: 2-(3,4-dimethoxyphenyl)-6-methyl-3-oxo-pyridazine-4-carboxylic acid

: 504-02-9
1,3-cylohexanedione

: 2222257-79-4
2-[{2-(3,4-dimethoxyphenyl)-2,3-dihydro-6-methyl-3-oxo-4-pyridazinyl}carbonyl]-1,3-cyclohexanedione

Guidance literature:: 2-(3,4-dimethoxyphenyl)-6-methyl-3-oxo-pyridazine-4-carboxylic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 17h; Inert atmosphere;

1,3-cylohexanedione; With triethylamine; In dichloromethane; at 0 ℃; for 0.25h;

With 2-hydroxy-2-methylpropanenitrile; In dichloromethane; at 20 - 40 ℃; for 22h;